Chemical Separation Process Operations
Principles of Equilibrium Staged Separation, Reaction Engineering, and Operational Discipline for Process SafetyBy Bethan Trelawny
Length15h 15m
About this audiobook
Design on paper. Start up at 3 a.m. This book teaches both.
A distillation column designed at total reflux on paper still has to be started up by someone at three in the morning. Chemical Separation Process Operations keeps both realities in view. It begins with the phase equilibrium behind every separation, then builds the equilibrium stage into binary distillation by McCabe-Thiele, shortcut multicomponent design, and real tray and packing hydraulics with their flooding and turndown limits. Absorption, extraction, evaporation, crystallisation, drying, membranes and adsorption each get a sizing method and a failure mode. Reaction engineering follows, from rate laws and reactor design equations to non-isothermal operation, multiple steady states and heat integration with the separation train. Closing chapters cover procedures, management of change and startup discipline.
Written for chemical engineering students and plant process engineers, the book connects fundamental theory to the equipment, procedures and operational decisions that determine whether a process runs safely and profitably. Each chapter pairs design methods with the practical limits that appear on the plant floor, so readers can move from a textbook calculation to a real operating window.
What you will learn:
• Select unit operations from process basis, feed conditions and product requirements
• Apply phase equilibrium thermodynamics to flash and staged separation calculations
• Design binary distillation columns using McCabe-Thiele and shortcut multicomponent methods
• Evaluate tray and packed column hydraulics, including flooding, weeping and turndown
• Size absorption, stripping, liquid-liquid extraction, evaporation, crystallisation and drying operations
• Apply membranes and adsorption to separation duties with their characteristic failure modes
• Use rate laws and reactor design equations for chemical reaction engineering
• Analyse non-isothermal reactors, multiple steady states and heat integration with separation trains
• Implement operational discipline, management of change and safe startup procedures
This book is for chemical engineering students, process engineers, and plant operations personnel who need a working understanding of equilibrium staged separations, reaction engineering, and the operational discipline that keeps process plants safe. Whether you are studying for a degree, designing a new unit, or troubleshooting an existing column at three in the morning, the material here bridges calculation and practice.
Audiobook details
GenreTechnology, Science and Nature
Length15 hrs 15 mins
Narrated byListen with 1,000+ voices
FormateBook with Audio
Publish dateSep 27, 2026
LanguageEnglish
Table of contents
1Chemical Separation Process Operations
2Foreword
3Preface
4About This Book
5Important Safety Notice
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6Chapter 1: Process Basis and Unit Operation Selection
71.1 From Client Brief to Block Flow Diagram
81.2 Separation Technology Screening and Selection
91.3 Material and Energy Balance Strategy for Separation Trains
101.4 Process Safety, Loss Prevention and Inherently Safer Design
111.5 Economics, Utilities and the Design Margin Question
12Chapter 2: Fluid Transport and Process Hydraulics
132.1 Line Sizing, Velocity Criteria and Pressure Drop
142.2 Pump Curves, System Curves and Net Positive Suction Head
152.3 Control Valves, Orifices and Relief System Hydraulics
162.4 Compressors, Vacuum Systems and Two-Phase Flow
17Chapter 3: Phase Equilibrium Thermodynamics
183.1 Vapor-Liquid Equilibrium Fundamentals
193.2 Activity Coefficient Models and Non-Ideal Systems
203.3 Relative Volatility, Distribution Coefficients and K-Values
213.4 Azeotropes and Their Consequences for Process Selection
22Chapter 4: The Equilibrium Stage and Flash Separation
234.1 The Ideal Stage and Stage Efficiency
244.2 Isothermal Flash Calculation
254.3 Adiabatic Flash and the Operating Line Concept
264.4 Stage Efficiency, Tray Spacing and the Ideal Stage Idealisation in Practice
27Chapter 5: Binary Distillation by McCabe-Thiele
285.1 Column Material Balances and the Rectifying Section
295.2 The Stripping Section and Feed Condition
305.3 Minimum Reflux, Total Reflux and the Operating Reflux Ratio
315.4 Optimum Feed Stage, Stage Count and Column Energy Balance
325.5 When McCabe-Thiele Fails: Constant Molar Overflow and Real Behavior
33Chapter 6: Multicomponent Distillation
346.1 Key Component Selection and Product Distribution
356.2 Fenske Minimum Stages and Underwood Minimum Reflux
366.3 Gilliland Correlation and Shortcut Column Design
376.4 Rigorous Stage-by-Stage Methods and Simulation Checks
38Chapter 7: Column Internals and Hydraulics
397.1 Tray Types and Their Selection
407.2 Flooding, Weeping, Entrainment and Turndown
417.3 Random and Structured Packing
427.4 Internals, Distributors and Column Auxiliaries
43Chapter 8: Absorption and Stripping
448.1 Solvent Selection and Dilute versus Concentrated Systems
458.2 The Kremser Method for Dilute Absorption and Stripping
468.3 Height and Number of Transfer Units in Packed Towers
478.4 Concentrated Systems, Desorption and Design Checks
48Chapter 9: Liquid-Liquid Extraction
499.1 Ternary Phase Diagrams and Tie Lines
509.2 Single-Stage and Cross-Current Extraction
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